96 Line TGA/STA-EGA

The highlights

Large volume & high temperature TGA/STA-EGA (ambient to 2000°C)

This is an extremely high performance weighing module used with the TGA 96. This balance can weigh samples up to 100 g and is well suited to measuring both micro-quantities of samples (a few milligrams) as well as large, dense samples while maintaining measurement resolution to within a microgram whatever the mass analyzed. 96 Line TGA/STA offers EGA temperature controlled coupling devices, enabling simultaneous heated capillary based MS, or GC/MS* connections

Simultaneous TGA-DTA/DSC measurements are available.

Simultaneous TGA-DTA: – Ambient to 1600°C, – Ambient to 1750°C, – Ambient to 2000°. Simultaneous TGA-DSC: – Ambient to 1500°C, – Ambient to 1600°C.

NEW PARTS AND OPTIONS
Pierced alumina crucibles
Alumina based crucibles pierced with numerous orifices to improve sample / gas interactions are available. 18mL and 4.5mL versions are available.

FTIR coupling
A heated MS or FTIR 200°C coupling was designed for the TG96 line.

Specifications
96 LineDTA 96DSC 96TGA
Temperature range of measurement module (C°)amb/1600, amb/1750, amb/2000amb/1500, amb/1600amb/1600, amb/1750, amb//2000
Volume of crucible (μl)220/550360/42018000
Max. sample size(mm)n/an/an/a
Resolutionn/a5μW0.3 μg
RMS noisen/a66 μW0,3 μg
Specific RMS noise n/a0,16 μW/μl0,016μg/ml
Measurement rangen/an/a+/-2000 mg
Evolved Gas AnalysisSimultaneous MS, GC/MS*

Thermostated interfaces up to 300°C

Features

In addition to the TGA 96, SETARAM proposes different accessories and software that permit, in particular:
– TGA measurements in corrosive atmospheres
– Controlled rate TGA measurement (CRTA: controlled rate thermal analysis)

Evolved Gas Analysis

96 Line offers temperature controlled coupling devices, enabling simultaneous MS, or GC/MS* connections. The coupling device is heated up to 200°C to avoid gas condensation and is completely insulated for a safe handling. 96 Line can be equipped on request with the state-of-the-art heated “Autoinjector” interface for TG-GC/MS* experiments.

*GC/MS is available on request.

Applications
Typical application areaMaterials
Gasification, pyrolysis, combustionCoal, biomass and wastes
Adsorption, desorption, calcinationCatalysts, sorbents, minerals
Dehydration, dehydroxylation, decarbonatationCements, minerals, ceramics, pharmaceuticals
Thermal stability, compositional analysisPharmaceuticals, polymers, cements, minerals, ceramics
OxidationMetals, alloys
Residual solventsPharmaceuticals
Polycondensation, curingPolymers
Documentation


Brochures

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