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Thermal analysis - DSC, DTA, TGA, coupling, TMA - calorimetry, gas sorption products

熱量測定

マイクロ熱量測定

マイクロ熱量測定

Microcalorimetry uses a suite of techniques to directly measure enthalpy and heat capacity changes that arise when chemical reactions occur. In aqueous solutions, heat flux into or out of the sample almost always happens on reaction. These reactions may involve a wide variety of situations, e.g., the interaction of two molecules (such as a cyclodextrin and its guest), changes in the conformation of complex macromolecules (such as proteins or DNA), or even in the structure of very complex multimolecular colloidal drug delivery systems (such as liposomes).


熱量測定

熱量測定

熱量測定


熱量測定は、制御された雰囲気中、温度が変化する条件で、試料の転移熱量を測定します。
色々なシステムを用意しています:等温、等方包囲、断熱、反応、滴定、溶液、落体式、Calvet-3D Sensor Inside 等


核廃棄物特殊化のための非破壊的な分析評

核廃棄物特殊化のための非破壊的な分析評

Calorimetry is the technique with the highest sensitivity for characterizing nuclear materials and waste.
When radioactive waste material in a container emits α and β radiation (e.g. from curium, plutonium, tritium, etc.) it also emits an amount of heat that is proportional to the quantity of radioactive material. This heat emission can be quantified using a SETARAM calorimeter.
SETARAM instrumentation's large-volume calorimeters (from 1 l to 90 l) can detect thermal radiation levels of just a few μW.


熱分析

示差走査熱量測定 (DSC) / 示差熱分析 (DTA)

示差走査熱量測定 (DSC) / 示差熱分析 (DTA)

DSC / DTA


DTA - 示差熱分析 - と DSC - 示差走査熱量分析 - は、それぞれ試料と参照試料(制御された雰囲気下で、同じ温度変化をすることが条件)間の温度差あるいは熱流差を測定します。
DTA は、全ての材料のあらゆる変化を検出し; DSC は、温度と伝達熱量を決定します。
セタラムは提案します:
- 全ての DTA システムで、高精度トライカップルプローブを使って、最も広い温度領域 ( -150°C ~ 2400°C°) ;
- ほとんど全ての DSC から選択 (品質管理用システムから最高感度 DSC や 3D-Sensor Inside DSC まで)
DTA / DSC  で測定できる特性には、相転移、ガラス転移、融解、純度、蒸発、昇華、結晶化、熱分解、比熱容量、重合、変成 / 集積、適合性等があります。


高圧示差走査熱量測定 (DSC) と 熱量測定

高圧示差走査熱量測定 (DSC) と 熱量測定

高圧 DSC と 熱量測定


高圧 DSC (または熱量計) によって、ユーザーは、1000 気圧! までの圧力下で材料や反応の解析が可能になります。セタラムのシステムでは、試料(容器、るつぼ)が入る測定チャンバーだけが圧力に曝されます。また、セタラムは、水素雰囲気で操作可能なガス制御パネルを設計しました。


熱重量測定 (TGA)

熱重量測定 (TGA)

TGA


熱重量測定 (TGA) は、材料の重量変化を測定します(制御された雰囲気中で温度を変化させる条件で)。
全てのセタラムの天秤は、最高の精度と安定性基準を満足しています。
熱重量測定 (TGA) で測定できる特性 には、腐蝕、熱分解、吸着 / 放散、溶剤損失、酸化 / 還元、水和 / 脱水、分解、カーボンブラック等があります。


熱重量測定と示差走査熱量測定 / 示差熱分析との同時測定

熱重量測定と示差走査熱量測定 / 示差熱分析との同時測定

STA または TGA - DSC / DTA


TGA-DSC:同一試料の TGA (熱重量測定) と DSC (示差走査熱量測定) の同時測定 を実行する時は、DSC プローブを天秤に装着します。
TGA と DSC 同時測定 - STA - は、別々の測定より多くの情報を提供します。
セタラムの製品には、ユニークな2400°C までの高温システムや対称型天秤と3D-Dimension DSC を結合した革新的システムが含まれています。


接続 / ガス分析装置

接続 / ガス分析装置

QMS または FTIR と接続した TGA


TGA( 熱重量測定装置 ) とガス分析装置 ( QMS : 四重極質量分析計、FTIR : フーリエ変換赤外線分光計、 GC : ガスクロマトグラフ等 ) との接続システム は、放出蒸気の同定や変質メカニズムの解析を実行します。
セタラムは、TGA ( 熱重量測定 ) とガス分析の最適な接続を目指して幾つかのシステムを開発しました:
- 超音波システム (SuperSonic System) は、MS 接続 TGA に、比類のない測定能力を提供します。
- キャピラリーシステム  は、ユーザーの TGA-MS や TGA-FTIR 測定を簡単に実行します。
他の熱分析装置も、GC、BET、や X-Ray 装置に接続され、良好な測定が実行されています。


熱機械特性分析 (TMA)

熱機械特性分析 (TMA)

TMA


熱機械特性分析 - TMA - は、プログラム温度中で、非振動応力下にある試料の変位を時間または温度に対して測定します。
縦型構造を持つセタラムの TMA システムは、試料に対して全く無視できるほど低い負荷から測定可能です。
熱機械特性分析 -TMA - で測定できる特性には、熱膨張率、軟化、焼結、ガラス転移等があります。


ガス湿度発生装置

ガス湿度発生装置

湿度 が、多くの材料の安定性に深刻な影響を及ぼすことはよく知られています。セタラムは、これらの影響を評価できるよう WETSYS 制御湿度発生装置 を開発しました。


ガス吸着

ガス吸着 HyEnergy, part of Setaram since 2008, is the industry standard in high performance Gas Sorption studies having developed the first high quality, high performance system (PCTPro) that could produce reliable, reproducible data for the different demands of hydrogen storage material.
Today that range has been expanded, built upon and improved to offer the world’s most fl exible, powerful and easy to use gas Sorption workstations in the market. Today’s systems offer even greater precision, whilst offering a unique level of fl exibility by allowing you to study liquids, solids, thin fi lms and sample sizes from mg to kg. We also offer the ability to work cryogenically up to 500 °C and with high pressure mass spectroscopy to measure off gases, and even symbiotic techniques with simultaneous calorimetry for a complete characterization of sorption processes.

熱伝導率

熱伝導率 熱伝導率熱拡散率 は、物質や組成の熱伝導特性を表す最も重要な熱物性パラメーターです。セタラムは、カナダのパートナー MATHIS 社の最新鋭熱伝導率測定装置 TCi を提案します。

SOFTWARE

熱解析ソフトウェア

熱解析ソフトウェア

CALISTO is a NEW softWare developed for Thermal Analysis applications from DSC, TGA, TMA and Calorimetry.


磁化飽和特性

磁化飽和特性

σs



強磁性体混合物の磁性特性は、機械的或いは熱的処理によって大きく変化します。専門家は、磁性特性のこれらの変化から、ある固相転移の進化を解析します。
磁性測定は、感度が高く、微妙な冶金学的現象の検出を可能にします。
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  • September 26, 2012 - September 28, 2012

    International Conference

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    Darmstadt, GermanyInternational Conference on Chemical Looping 201226th to 28th of September 2012A Concept for Efficient and Clean Use of Fossil ResourcesThe Institute for Energy Systems and Technology (EST) at Technische Universität Darmstadt is pleased to announce the 2nd International Conference on Chemical Looping as „An Alternative Concept for Efficientand Clean Use of Fossil Resources”, to be held from Wednesday 26th to Friday 28th of September 2012 at Maritim Conference Hotel Darmstadt.
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    Edinburgh, UKMOF20123rd International Conference on Metal-Organic Frameworks and Open Framework Compounds September 16, 2012 - September 19, 2012John McIntyre Conference Centre, Edinburgh Dechema and the IZA together with the local organising committee warmly invite you to attend MOF2012 in Edinburgh.The aim of MOF2012 is to address all questions concerning the community working with metal-organic frameworks, metal coordination compounds and related materials covering all aspects of MOFs from synthesis and characterization of new materials over properties of MOFs to all kinds of applications, e.g. in biology/medicine, catalysis, magnetism, luminescence and adsorption. We are looking forward to experimental, theoretical, and modelling contributions along with papers addressing key questions regarding potential industrial applications of this fascinating family of materials.
  • August 20, 2012 - August 24, 2012

    ICTAC 2012

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    Osaka, JapanICTAC 201215th International Congress on Thermal Analysis and CalorimetryAug. 20-24, 2012 Kinki UniversityInternational Congress on Thermal Analysis and Calorimetry (ICTAC) is held every four years, with an aim to promote international understanding and to exchange ideas and findings in the field of thermal analysis and calorimetry.  In 2012, memorable 15th ICTAC is held in Osaka, Japan. Osaka is located virtually in the center of Japan, and is near to ancient and beautiful cities of Kyoto and Nara.
  • August 12, 2012 - August 15, 2012

    NATAS 2012

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    Orlando, Florida, USA40th Annual Conference of NATAS Technical ConferenceAugust 12-15, 2012Short CourseAugust 10-12, 2012Buena Vista Palace Hotel & SpaWith great pleasure, we invite you all to the 40th Annual Conference of NATAS that will take place in Orlando, Florida, 12-15 August 2012.
  • August 05, 2012 - August 10, 2012

    ICCT 2012 and CALCON 2012

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    Búzios, BrazilICCT 2012 and the 67th Calorimetry ConferenceWe are delighted to invite you to take part in an event that that is unique in every way: the association of ICCT 2012 and the 67th Calorimetry Conference, being held together, both for the first time in Latin America.
  • July 15, 2012 - July 19, 2012

    INMM

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    Orlando, Florida USAINMM 53rd Annual MeetingJuly 15-19, 2012Renaissance Orlando Resort at SeaWorldOrlando, Florida USAThe 53rd Annual Meeting will provide attendees with a professional forum for the exchange of the latest technical information in nuclear materials management. The meeting will address all aspects of nuclear materials management with papers and posters organized by the INMM Technical Program Committee.
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    BZA 2012

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    Chester, EnglandThe 35th Annual British Zeolite Association Meeting15th - 20th July 2012University of Chester in northwest EnglandThe 2012 meeting of the British Zeolite Association will be held at the University of Chester in northwest England. This triennial, Chislehurst-style BZA meeting, organised along the lines of a Gordon Conference, will be limited to 120 participants.The BZA welcomes contributions from all fields of zeolite, microporous and mesoporous materials science, including synthesis, structure, applications, characterisation, catalysis and computational studies.
  • June 26, 2012 - June 29, 2012

    CTEC 2012

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    Lyon, FranceCalorimetry and Thermal Effects in CatalysisCalorimetry and thermal analysis methods, alone or linked to other techniques, applied to the characterization of catalysts, supports and adsorbents, and to the study of catalytic reactions in various domains: air and wastewater treatment, clean and renewable energies, refining of hydrocarbons, green chemistry, hydrogen production and storage, CO2 capture...
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    Milano, Italy20th European Biomass Conference and Exhibition18 - 22 June 2012 at the Milano Convention Centre in Milano, ItalyWith this event, we will continue the biomass specialist's role as the leading technical platform covering all aspects of biomass from research to industry and markets.
  • June 05, 2012 - June 08, 2012

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    Rome, ItalyAICAT 2012Sapienza University of RomeJune 5-8 2012AICAT 2012 is jointly organized by the Italian Association of Calorimetry and Thermal Analysis (AICAT) and by Interdivisional Group of Calorimetry and Thermal Analysis (GICAT) of the Italian Chemical Society (SCI) and represents the main scientific meeting of these Associations. The Congress aim is to provide to the scientists working in Calorimetry, Thermal Analysis and closely related topics an opportunity for an exchange of scientific information, critical discussion and advanced planning on fundamental and applied research aspects of interest in this field.
  • May 28, 2012 - June 01, 2012

    2012 Fiery Ice

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    Sapporo, Hokkaido, Japan2012 Fiery Ice8th International Workshop on Methane Hydrate Research & DevelopmentWith great pleasure, we announce that 8th International Workshop on Methane Hydrate Research & Development (Fiery Ice from the Seas) is being held in Sapporo, Japan at refreshing season, 28th of May to 1st of June, 2012.
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    Siófok, Lake Balaton - Hungary BiPoCo 2012,an International Conference onBio-Based Polymers and CompositesMay 27-31, 2012Siófok, Lake Balaton - HungaryDownload the First circular
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    Toulouse, FranceThe 43rd Calorimetry and Thermal Analysis DaysMore information coming soon
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    Les Embiez, FranceHTCPM 20128th International Symposium on High-Temperature Corrosion and Protection of Materials20 - 25 May, 2012Les Embiez, France The goal of this international symposium is to reflect the interests of the major industries dependent on the successful application of high-temperature materials, providing a periodic updating on the current research and understanding in these areas.
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    Lleida, SpainINNOSTOCK 2012The 12th International Conference on Energy Storage16-18 May 2012Innostock 2012 is part of the Stock conference series sponsored by the ECES IA of the International Energy Agency.Innostock 2012 will gather the world’s leading specialists and academic researchers within the field of energy efficiency through energy storage. Energy storage will present in all its topics:• Underground thermal energy storage• Sensible, latent and thermochemical energy storage• Electrical storage
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    11th International Hydrocolloids Conference

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  • April 30, 2012 - May 03, 2012

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    Pittsburgh, Pennsylvania - United States 11th Annual Conference on Carbon Capture Utilization & Sequestration April 30 - May 3, 2012Pittsburgh, Pennsylvania The 2012 Conference program follows in the footsteps of the past 10 events, with an added emphasis this year on potential utilization of anthropogenic carbon emissions that is reflected in the new name of the conference. The focus is on systems and technologies that are being or could be deployed in the U.S. and North America.
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    Copenhagen, DenmarkFood Colloids 2012This conference is the fourteenth in the series of biennial European conferences dedicated to the area of food colloids. Food Colloids is a highly multidisciplinary topic that brings together scientists from many different areas. The aim of the conference is to present the state of the art on a number of fast evolving questions and to promote discussions and interactions between researchers involved in different fields of food colloids. This series aims to emphasise the importance of approaching the subject from different perspectives; from the fundamental physical-chemistry to the nutritional and consumer aspect of the food product.
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    TAC 2012

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    The Royal Society of ChemistryThermal Methods Group presentsTAC 20123 - 4 April 2012Food Sciences DivisionSchool of Biosciences, University of Nottingham, UK
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  • March 18, 2012 - March 23, 2012

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  • February 27, 2012 - February 29, 2012

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    Doha, Qatar | W Doha HotelApplied Gas Hydrate Management (Challenges and Opportunities)27 – 29 February 2012This workshop has the objective of bringing together a range of industry, academic and government professionals into an environment where they can brainstorm, troubleshoot and discuss the fundamental understanding of all aspects of hydrate management. Part of the workshop will be discussions on hydrate management, including sweet and sour gas application, the impact of facilities design, removal of KHI from produced water, applications of treatment chemicals and the use of novel methods to control hydrate problems.
  • January 31, 2012 - February 04, 2012

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